Main results obtained by J.L. Marignier                                           
      in the reconstruction of the photographic                              
      processes invented by Nicéphore Niépce (1765 - 1833)

Laboratoire de Chimie Physique UPS/CNRS Orsay - FRANCE     


      The World's first photograph at Austin TX - USA     The Images shown by Niepce in England              
       The Discovery of the Physautotype process              The reconstitution of the Table Servie
  

    Première            first photograph            Moonlight          Ruis of an abbey           Table servie
           
 -
        Heliography           Physautotype            The world's first photograh              Ruins of an Abbey
            La Table Servie            Virtual Niepce's House
-

Heliography

First images obtained in 1989

Helioengraving process

Helioengraving process described by Niepce as : "to paint and to engrave alternatively"

The world's first photograph made by Niepce, at the University of Texas - AUSTIN  USA (July 1990)

The bitumen mines


Discovery of a drawing used by Niepce

The three plates in England


Technical studies about the bitumen process


Physautotype

Discovery of the physautotype process


La Table Servie



Others

Processes using powders

The unsuccessful attempts made by Niépce


Computer analysis

Virtual Niepce's House

Virtual reconstruction of the world's first photograph






















Heliography

First images obtained in1989

Helioengraving process

Helioengraving process described by Niepce as : "to paint and to engrave alternatively"

The world's first photograph made by Niepce, at the University of Texas - AUSTIN USA (July 1990)

The bitumen mines

Discovery of a drawing used by Niepce

The three plates in England


Technical studies about the bitumen process


Physautotype

Discovery of the physautotype process


La Table Servie



Others

Processes using powders

The unsuccessful attempts made by Niépce


Computer analysis

Virtual Niepce's House

Virtual reconstruction of the world's first photograph





















Heliography

First images obtained in1989

Helioengraving process

Helioengraving process described by Niepce as : "to paint and to engrave alternatively"

The world's first photograph made by Niepce, at the University of Texas - AUSTIN USA (July 1990)

The bitumen mines

Discovery of a drawing used by Niepce

The three plates in England


Technical studies about the bitumen process


Physautotype

Discovery of the physautotype process


La Table Servie


Others

Processes using powders

The unsuccessful attempts made by Niépce


Computer analysis

Virtual Niepce's House

Virtual reconstruction of the world's first photograph






















Heliography

First images obtained in1989

Helioengraving process

Helioengraving process described by Niepce as : "to paint and to engrave alternatively"

The world's first photograph made by Niepce, at the University of Texas - AUSTIN USA (July 1990)

The bitumen mines

Discovery of a drawing used by Niepce

The three plates in England


Technical studies about the bitumen process


Physautotype

Discovery of the physautotype process


La Table Servie



Others

Processes using powders

The unsuccessful attempts made by Niépce


Computer analysis

Virtual Niepce's House

Virtual reconstruction of the world's first photograph



















Heliography

First images obtained in1989

Helioengraving process

Helioengraving process described by Niepce as : "to paint and to engrave alternatively"

The world's first photograph made by Niepce, at the University of Texas - AUSTIN USA (July 1990)

The bitumen mines

Discovery of a drawing used by Niepce

The three plates in England


Technical studies about the bitumen process


Physautotype

Discovery of the physautotype process


La Table Servie



Others

Processes using powders

The unsuccessful attempts made by Niépce


Computer analysis

Virtual Niepce's House

Virtual reconstruction of the world's first photograph







Heliography

First images obtained in1989

Helioengraving process

Helioengraving process described by Niepce as : "to paint and to engrave alternatively"

The world's first photograph made by Niepce, at the University of Texas - AUSTIN USA (July 1990)

The bitumen mines

Discovery of a drawing used by Niepce

The three plates in England


Technical studies about the bitumen process


Physautotype

Discovery of the physautotype process


La Table Servie



Others

Processes using powders

The unsuccessful attempts made by Niépce



1989 to 1992

HELIOGRAPHY



First images obtained in the camera obscura using the process invented by Niepce, since his death in 1833 

The images was obtained by the most sophisticated form of the invention of Niepce that he described in 1829, i.e. on silver plated copper plate with the process of inversion of the negative asphalt image by the action of iodine vapors.
           
After this first success, it was possible for the first time :
• to determine the photosensitivity of the system (few 10-6 ISO) and hence of the exposure time
              (3 days under the sunlight with an aperture of the lens of f/4).
• to demonstrate the absence of any whitening of the asphalt under the action of light.
• to determine the resolution of the image (102 pairs of lines per millimeter).
• to show that the process gives black and white images with a good gradation of hues.

Discovery of the possibility to produce on pewter (Sn), bitumenfirst heliograph images which can be seen as negative or positive depending on the orientation of the light. 
• taking into account one sentence written by Niepce in his "Notice sur l'Heliographie" : suggestion that Niepce could have obtained such kind of images (catalog of the exhibition at the Nicéphore Niépce Museum, published on 15 th december 1989)
• Images on glass and on lithographic stones (limestone) which exhibit the same phenomena
                                                                                                        Heliograph made in a camera obscura
using the process invented by Niépce
(J.L. Marignier 1989)


Reconstruction of the helioengraving process

           • Images etched with acid in copper or pewter (Sn) plates
           • Prints of these images on paper


=>These very first results have been presented at the Symposium for 150th anniversary of the birth of photography at Vevey (Switzerland) in july 1989
=>The images have been exhibited in October-November 1989 at the Archives Nationales in Paris and then at the Nicephore Niepce Museum in Chalon-sur-Saône from 15th december 1989 to 15 th march 1990. These heliographs are still in the archives of this museum.



     
Reconstruction of the helioengraving process with the techniques described by Niepce as : "peindre et graver tour à tour" (to paint and to etch alternatively)




    
Observation of the world's first photograph made by Niépce, at the Harry Ransom Humanities Research Center (HRHRC) at the University of Texas - AUSTIN USA (July 1990)

• First determination of the nature of this image :First photograph it is a negative/positive bitumen image made on pewter (Sn). The bitumen used by Niépce is still onto the pewter plate. This confirms the suggestion we proposed in 1989 and hence our good interpretation of the "Notice sur l'héliographie". Due to an underexposure of the image in the camera obscura the bitumen varnish is completely eliminated in the dark areas but also partially dissolved even in the most intense areas. It is known that in the engraved images on metal, this dissolution can lead to a discontinuous structure of the remaining varnish called "sablé", i.e. "sand effect", by A. Lemaître, the engraver who collaborated with Niépce (published in 1990 and 1999). In these conditions the exposure lasts 2 days under the sunlight.

The oldest world's photograph as reproduced
by Kodak in 1952



After this it has been possible to date the "View from the window at Gras" as made by Niépce during summer 1827 and not in 1826 as it was written before.

First photograph Gernsheim                      First photograph by Marignier
                     The image made by Niepce as it was in 1952                          Image made by J.L. Marignier






August 1993 : Investigations in the now closed asphalt mines where Niépce had purchased the bitumen.
               
          • Extraction of the bitumen from 15 kilograms of bituminous ore and production of heliographic images              with it.





April 1995 : Discovery at the Musée du Cinéma in Paris of an unknown varnished drawing on paper used by Niépce
                  
Niepce in England Drawing• It represents the image which can be seen on the plate called "Ruins of an Abbey" now preserved at National Media Museum, Bradford, UK. This drawing covered with a varnish to make the paper translucent is absolutely identical to an engraving preserved at The George Eastman House on which one can read that it is a reproduction of an painting from Daguerre by the engraver G. Maile and that the true titled is "Un clair de Lune", i.e. "Moonlight". Details and dimensions of this drawing corresponds exactly to the image on the plate in UK and this leads to the conclusion that this varnished drawing was reproduced by Niepce by contact printing and not with a camera obscura (published in 1999, ed. Belin p. 494), which seems obvious because Niépce would not have varnished it.

Niepce in England GEH Rochester
This photograph shows the engraving preserved at the George Eastman House (Rochester NY USA). This is an engraving on which one can read "Dessiné par Daguerre" et "Gravé par G. Maile", dimensions and details are identical to the drawing in Paris and to the plate in England (see after for the comparison)















November 1997 at the Royal Photographic Society, Bath, UK. Observations of the three plates shown by Niepce in England in 1827
           
Ruins of an abbey Bradford - Niepce in England



• Observation of the image : "Ruins of an Abbey", which is the reproduction of the "Un Clair de Lune", gives rise to some questions about the plate and the process used. The aspect is the reverse of the one expected for an engraved image by Niepce's process. Dark areas are very naked polished metal while the area of intense light are matte. While the metal is a white bright one it is not sure that it is a pewter (Sn) plate. In 1999 (Ed. Belin), I suggested to perform analysis of the metal and of the different areas.







Ruins of an Abbey : the plate  preserved in England
    Ruins of an Abbey Bradford NMM Niepce in England                Niépce. L'invention de la photographie. Niepce in England
 In 1999, J.L. Marignier showed in his book, the connection between the engraving in Rochester, the plate in England, and the drawing on paper he discovered at the Musée du Cinéma in Paris

Comparison Bradford Paris - Niepce in England
Comparison between the drawing discovered at the Musée du Cinéma (Paris) and the plate in Bradford museum (on the drawing, look at the pinhole on the top left angle which is reproduced on the pewter plate)




Technical studies about the process

• Solvent extraction of the chemical components of the bitumen.                  
          • Study of the photosensitivity of the different components.
• Study of the effect of the concentration, the temperature during the dissolution, the stirring during the       dissolution, the temperature of drying, the ageing of the solution, the thickness of the bitumen film.
• Study of the effect of the reflectivity of the base.
• Determination of the spectral sensitivity of the bitumen film. 




1992 to 2004

PHYSAUTOTYPE


Re-discovery of the unknown photographic process using the residue of the distillation of oil of lavender (feb 1992)

• Analysis of the letters between Niepce and Daguerre leads to the conclusion that this process was invented by Niépce and Daguerre together during summer 1832.
• Identification of this process as the one called "PHYSAUTOTYPE" by Niépce and Daguerre in their correspondence in 1832.
• In 1993, discovery that the same process can be implemented also with rosin and a lot of aromatic compounds.


Identification of the image called "La Table Servie" as a physautotype made by Niepce in 1832 - 1833

Table Servie Jardin Niépce
1995 : Discovery in the travel diary of James
David Forbes (Scotland) in 1839 that he was a witness of the image called " La table servie" which he saw in the hands of the son of Niépce, Isidore Niépce in Paris. This testimony leads to attribute without no doubt this image to Niepce. And a careful analysis led to conclude that this picture was taken using the physautotype process.
2003 : Discovery of another witness of the image of " La table servie", the russian academician Joseph Hamel.
• 2004 : reconstitution of the " Table servie" in Niépce's garden at Saint-Loup-de-Varennes by the physautotype process.
                                                                                                                   Reconstitution of Niepce's Table

   Table Servie 1902                Table servie Physautotype
Left : reproduction published in 1902 of  Niepce's plate (At present day, the plate is lost) . Right : Physautotype made by J.L. Marignier and M. Lourseau with a camera obscura of the reconstituted table of Niépce (August 2004)

Processes using powders
Discovery that under the influence of Daguerre, two processes have been derived from the heliographic process and from the physautotype process.


Two example of images obtained by contact printing on powders spread on metal. Left : powder of bitumen on silver. Right : powder of colophony on silver.
 
1995 to 2004

THE UNSUCCESSFUL ATTEMPTS AND PROCESSES ACHIEVED BY NIEPCE FROM 1816 TO 1820


Reconstruction of the experiments performed by Niepce before the invention of the bitumen process

• Images made by Niépce in 1816,using the silver chloride precipitate, and called by him : retinas.
• Images made with iron chloride.
• Images made with guaiacuum resin.




1992 to 2004

VIRTUAL RECONSTRUCTION OF NIEPCE'S ESTATE


Reconstruction with a computer of Niepce's estate as it was in 1830
 
• Identification of the window from where was taken the world's first photograph
• Determination of the position of the camera obcura.
• Determination of the focal distance of the lens used.
• Identification of the details of the image.
Calculations indicate that, since 1827, the window has been shifted toward the west by 70 cm.
=> Publication of these results in september 1999 (Ed. Belin).


• In december 1999, investigations around the window in Niépce's house confirm that it has been shifted since the time of Niepce and that the shift is exactly of 70 cm. (results presented in the movie "Restoration of Niépce's house" in 2000)
=> Results presented in the movie "Restoration of Niépce's house" Spéos-SCAVO-CNRS, 2000.



Virtual reconstruction of the "View from the window at Gras"


• Calculation with computer of the shadows of the landscape at every hours of the day for any day of the year.
• Reconstitution by computer of the world's first photograph, by calculating the accumulated intensity of the light produced during one day by the image projected inside the camera obscura on the plate.
• Determination of the period of the year (around the 15th of July) where this picture was made in 1827.
=>
Results presented at the Symposium on the world's first photograph at
the Harry Ransom Humanities Researches Center - Austin - Texas in November 2003.